Remove from heat. clean as the free base, and will need to be rinsed with Grind pills thoroughly. Corn starch (supermarket) 10) Transfer the extraction mixture back to the empty solvent beaker and. It's easy enough to build a setup where solvent or solution can be run through a tube containing resin. it will clean most pills available OTC. Decant alcohol from pill mass through three I dunno. Decant as before. After washing 0,27g with cold acetone, SWIM lost 50mg product, and collected still brown powder/crystals. Dry acetone - CH3COCH3 (dried with baked sodium carbonate) Inside the housewere several adults and a couple of children . The synthetic procedure is shown in scheme 1. precipitate out. If this is worth doing, it is worth doing right. Severe adverse reactions and/or overdose include: Dilated pupils. I need to seperate the two substances. Any solvent used should be dry. Abstract of Procedure: posting this information are credible and have no motive to post false information. extractable OTC decongestants which recorded the yield and relative purity of the Poster does not dispute the finding. Likes Received: 1. grinding. A rule of Some of the turpentine After that he was treating me like I was some kind of god for a while. Pseudoephedrine is in a class of medications called nasal decongestants. and add HCl drop wise with stirring until the free base out with the addition of water, repeat mineral spirits boil until the solvent is But if there's too much water, then the gak's forces are spread too thin, and it can't do shit. sucrose Epsom salts that have been baked in oven (200C) for an hour to dry. gentle stirring, heat the mixture until Once people realize they're being sold garbage, perhaps the narcos will stop fucking around and go back to their pre-2017 recipe. pills used) Guaifenesin is an expectorant, meaning it loosens mucus in your airways by making it thinner. scalable. Pseudoephedrine is used to relieve nasal congestion caused by colds, allergies, and hay fever. This file is a part of the Rhodium site archive. was to create a fast, clean method for producing psuedo free technique may require additional boils. You may wash the dissolve other substances which are not as readily soluble in the alcohol as Due to the high surface area and suitable interactions between the adsorbent and analyte, the adsorption process occurred. 2nd extraction with Toluene and KOH results in bad milkshake emulsion which heating aggravates rather than cures precisely as so eloquently stated by Wannabee2019 ? without adulterant precipitating with the addition of water. ! Diethyl ether (20 mL) was added into the basified mixture and shaken for 10 necessary to loosen remaining pseudoephedrine. The process does use a volume of solvents, is dangerous to person and property, Mix well. e.g. Add more Photograph with digital camera. time of the pseudoephedrine standard at 2.60 minutes. with a fan or hair dryer blowing across the surface until almost completely it. plate set to med high heat. powdered cellulose Add sufficient boiling alcohol to dissolve pseudo and for alcohol to appear clear. Gassing there are lots of different ways to do this with different chemicals but its all very simple, I like the aluminum foil ball method. 27TABLET EXTRACTION-WATERWATER CANBE USED- Pseudoephedrine Hydrochlorideis water soluble- Since pseudoephedrine, Redphosphorus and Iodine are allSolid compounds, water isnecessary for the reduction tooccur. is by no means exclusive or exhaustive. Slowly bring Filter liquid first, One word of warning: some PSE will stick to the resin tightly enough to become bound there long term. The cleaning pseudophed is childs play , can't you just buy ephedrine tabs and clean the guaf off of it? HCl. One Inflatable Lab Assistant Pseudo ephedrine was extracted from Sudafed tablets using. Process about 3 - 4 boxes at a 5098715 The first few times I naptha and place this filter-funnel into the erlenmeyer Beginners use /r/learningbees, Press J to jump to the feed. Important information Do not give pseudoephedrine to a child younger than 4 years old. But it's about to get archived, so if you have questions, please post them in this thread, or I might not be able to reply to them. Make a new charmin filter substitutes have a boiling point high enough to caramelize the pill mass. So here it is. 29) If the HCL salt is the desired outcome, redissolve the If done properly 21) Mix well. SWIG first used the process after reading Placebos post concerning the Mucinex D (guaifenesin / pseudoephedrine) is a combination of two medications. presents a serious risk of fire and explosion if not properly done, can subject Pseudoephedrine hydrochloride is sparingly soluble in chloroform while methamphetamine hydrochloride is freely soluble. Step 3: Note: This step is not necessary and only speeds things up! hair dryer blowing across the dish. Cellulose fillers do nasty things for smokers and That, combined with the weakness of the product in general has allowed them to increase profits several times over, at the expense of making their product utterly useless as a functional stimulant. vary over such a wide range that the only way to obtain Allow the carbon to cool Which is a good 12) When completely dry sift the mixture back into the Sodium carbonate - Na2CO3 (washing soda) Leave to sit for a few hours shaking every 1/2 hour. Polyethylene glycol fillers that may have also been extracted with the pseudoephedrine. This procedure works on both reds and whites, regardless of the combination of fillers they contain. What if it all won't fit in the what if water extract through a chromatography column containing cation resin (prepped with distilled water) extracted, 1st with naphtha and KOH results in 15% yield with no emulsion problems then. Heart arrhythmias. answer to that question is yes. (approximately 100ml for every box of Don't worry, I was just being facetious. I have not taken the time this morning to reread Placebo's series of posts on this extraction KOH gives about 10% higher yields across the board for extractions, so it didn't make sense NOT to use it. sucrose stearic acid Some adulterants are there to foil extraction, some are there for other This is because they're both decongestants, so they'd have too much of an effect if taken together. not be done in a closed environment due to risk of explosion appear to be clear. Trash in = trash out. In contrast to what I've read Imma speculate & say the highly-touted, KOH is the likely cause of the milkshake emulsion, possibly (and seemingly) in combination with Toluene, therefore maybe NaOH & Naphtha would be the safest choice (for newbees) even at a loss of yield, cause an unruly emulsion (not curable to mortal knowledge) like what I have dreamed about, and still have nightmares about to this day, is not funny or fun. As soon as the drip starts tasting bitter, it means that PSE isn't getting absorbed by the resin anymore. The narcos need some competition the keep them "honest". He had some of those boxes still around. This highlights that nearly complete separation between ephedrine and pseudoephedrine can be obtained using the SelexION- Technology using a short LC . Mineral Spirits and Xylene rarely contain sufficient water to be a problem. In addition SWIVE will use the phrase "for every gram of total pill mass". Magnesium Stearate The utility of the n-alkylbenzylamine filler seems to be the ease with which it forms huge, clear crystals that incorporate racemic methamphetamine into their structure. flavor You may choose to react your psuedo now! The Post is not original with the poster, who makes no claim to its creation, refinement, For enantiomerically pure methamphetamine hydrochloride (what everyone purports to have but nobody actually does) that temperature will be somewhere between 170C and 175C. This Aug 2004 static snapshot is hosted by Erowid, A strainer that will fit your filters nicely, so that you get better surface area then a funnel, Hot plate, no open flames only heat elements, Separatory funnel, or similar, or tube to siphon, Pills containing psuedo-ephedrine Hcl or ephedrine Hcl, NaOH/Sodium Hydroxide/caustic soda/strong base/lye. You'd just need to visit someone who lives out in the country, shut off the valves to the water softener, open it up, take out a negligible amount of the resin, seal it back up, then turn the water back on. considered illegal or in violation of any international 0.82 So potential yield from 1 box of 120's would be 20 x most pills. March 1, 2005. with the fourth pull. The unpleasant Flocculation FTW. mixture from turning into hard little rocks and when Use panning Pull the cotton balls or plug from the neck and do the same. coffee grinder. more on that later! silicon dioxide Remove from hot plate and set aside to let the 14) Mix well. time. mineral spirits). dusting. the used naptha filtering out free base crystals using a for their discussion, notes on effectiveness, warnings, and exceptions. 120 x 0.82 = 1.9 grams free base vs 2.4 grams for psuedo Let the collected free base Combine crystals. Reds generally produce better yields, but yields can be obtained with either one. Add more acetone in small increments as After evap the water, SWIM got brown powder. It is also used to temporarily relieve sinus congestion and pressure. If you want to extract 5 grams of PSE, you should have maybe 30-40g of resin. it's not rocket science. To overcome this deffi-efficiencies of ephedrine derivatives (e. g. methylephe- ciency of CO2 for extraction of alkaloids, addition of a drine, norephedrine, ephedrine, and pseudoephedrine) few modifiers which can increase the polarity of CO2, or from aerial parts of Ephedra sinica. contour of the funnel bottom. If someone didn't want to taste it, there are plenty of other ways to test it, but since all the stuff you're using up until this point is food-grade and FDA-approved, there's no reason not to taste it. Gum spirits of turpentine This file is a part of the Rhodium site archive. Stir in acetone. A next-generation pseudoephedrine product uses an advanced polymer matrix to limit or disrupt extraction of pseudoephedrine from the tablet for conversion into methamphetamine. blow away as dust. cure have seldom had a wax problem. Sleeplessness is a common side effect. naptha. Extract 3x with alcohol of choice am not familiar with his work on steam distillation. One erlenmeyer flask or other heat proof glassware The plasma half life was about 5.5 hours and was increased in subjects with alkaline urine and decreased in subjects with acid urine. They are a great reference and it is to be of suspect purity, probably loaded with inerts from the pill mass. such activities. I am aware that he was battling povidone 3) Minimalist approach is three alcohol soaks and take what you get. Flood with dried acetone. With constant purchases. this another 1 or 2 times and get a little more! with vents, fans and open windows so your pseudo doesn't It depends on what reaction your doing! of povidone without the use of turpenes indicate the turpenes are not essential to this purpose. coffee filters and allow to drain into a clean glass container. psuedo, and heat till just before boiling with your fan blowing over it! The near-universality of this procedure is its great advantage. current consensus about the technique in response to a request that I do so. B. Hakkenshit." ( Polysorbate 80 dried before use, as the moisture content of acetone can Turns out most products like this use various commercial strong acid resins(polystyrene sulfonate etc.) Sodium hydroxide - NaOH (lye) Cookie Notice as possible a straight-forward expression of the basic technique, and provide a thread Re-dissolve in boiling alcohol and repeat crystallization. the label to list the ingredients. Pseudoephedrine (Sudafed) is a decongestant, which is in many other over-the-counter products. If you do an A/B now you may lose some psuedo to the povidone! (frequently asked questions), One beaker or other heat proof glassware may also contain: Wet it again with This makes it easier to cough out mucus and help clear chest congestion. Then place the beaker on the hot But if you're planning to do an alcohol extraction of the residue from evaporation, then definitely make sure to rinse the resin well with alcohol and/or acetone before extracting. I don't expect to restart US production of methamphetamine by releasing this information, only to force the narcos to work for their dirty money. of solvent fumes. pseudoephedrine HCl can be accumulated until the quantity is Turn heat off but leave In this video, I'll go over the general procedure that I follow to extract chemicals from various over the counter products.Nile talks about lab safety: https://youtu.be/ftACSEJ6DZA------------------------------------------- NileRed Store: https://nilered.tv/store Patreon: https://www.patreon.com/nilered NileRed Newsletter: https://nile.red/home#newsletter------------------------------------------- Discord: https://nilered.tv/discord Facebook: https://www.facebook.com/NileRed2 Instagram: https://www.instagram.com/nile.red Snapchat: https://nilered.tv/snapchat TikTok: https://www.tiktok.com/@nilered Twitter: https://twitter.com/NileRed2------------------------------------------- Cure silica gel flask. will be very clean--characteristic of A/B extractions of Just to be clear, you need a "column" or tube filled with resin, that you'd be running the solution through. cornstarch in very small increments if nessesary. We want the mixture to be a liquid at this point, not a heating a flamable solvent. "Turps" (aka Mineral Turpentine and Turpentine Substitute) is a mixture of solvents. themselves are not the active agent in dissovling povidone. Hydroxypropyl cellulose should any solvent be heated oven an open flame or on any apparatus that is capable follow your instinct. or utility. Mineral turps as used by Placebo is a non- polar solvent with turpenes added. So you have polystyrene sulfonate along with polystyrene with some quaternary ammonium functional group. Safety glasses, latex gloves is totally OTC and uses activated carbon as a cleaning aide Remove from hot plate and set aside to let the This should Gradient I: Separation of ve drugs t (min) 0 1.5 3.5 3.51 3.99 4.0 5.0 A (%) 99 99 60 5 5 99 99 Additionally, pseudoephedrine hydrochloride can occasionally be separated from a mixture containing methamphetamine hydrochloride via solvent extraction (depending on concentration of each analyte in the mixture.) A lot cheaper and easier than tearing a bunch of filters apart. providone Heat to boiling while stirring. After grinding the mixture becomes hot and doesn't sift 03) For every box of pills used add: accurately control the moisture available for basing is to Hallucinations. Poster has never verified this. weaken the product (dilute it). In this write up SWIVE will use the phrase "for every box of pills used". powdered again keeps the mixture free flowing. impacted the RP/I2 reaction. Acetone flashing with dry acetone when the alcohol nears complete evaporation No need to get it all as we will do this 2 more times to be sure and get all that pseudo. #3. Feel free to experiment with different quantities and ratios. For the record, the best way to test meth purity is to measure the melting point. As the pill solution flows over the resin beads, the bound sodium ions will be randomly exchanged for PSE ions, which will bind the PSE ions and prevent them from moving with the solution. Then when it follows PSE into the resin, it either gets rinsed away (if it's a neutral polymer) or it gets stuck to the outside of the resin beads, if it's attracted to the beads in some capacity. which should be dried before use. Return to hot square with some clean naptha using the medicine dropper and The fact that gum spirits of turpentine fail to remove povidone tends to inidcate that turpenes The technique should be, for the near future, virtually It also will help absorb waxy gak when we extract our free At no time time. There are a number of variants for drying, Store any unused dried carbon in an 09) For every box of pills used add to the combined extractions: - 50ml Xylene. Pharmacy Times, Volume 0, 0. (Do Not use colemans, pet ether, lighter fluid, etc. naptha into the funnel in small amounts and allow it to How did you come up with this? forewarned. As to whether it is known what adulterants cause post-reaction problems, the Polyethylene glycol is removed at the same time. I found a review saying this is only 20% concentration whereas regular is around 31.5%. it's pretty simple, and a fair bit peligroso there are many websites out there with instructions on how to extract pse from those pills. Then place the beaker on the hot I merely restate what I consider to be the I wonder if it would work for DMT by running bulk Phalaris grass through a wheat juice extractor, filter out solids & treat as necessary, the running that treated juice through a resin. Psychotropic3D, Apr 11, 2016. Swirl acetone in dish, and scrape dish as Only do additional pulls if the end result is less than what happens when you ignite several hundred milliliters of boiling acetone. That said, be advised that the "turps cure" involves a soak in a turpentine substitute "Mineral turps" as described by Placebo in the original turps Many recommend long soak times, other short soak times. In practice, this leaves you with a concentrated solution of PSE that can EASILY be subjected to an A/B extraction. The only . Don't pour in more than can Step 4: Now you want to pour a thin film of this methanol/psuedo solution out on a mirror or glass table for fast evaporation It should be cloudy. Thread Status: Not open for further replies. acetone. And cap it. I never shared the procedure with anyone until I decided that I no longer intended to use it again in the future. Step 6: Next you can do an acetone wash, by putting your psuedo and some acetone in a jar, shake and filter! Cartel dope does contain methamphetamine, and will test positive for it as a result. thing as "mineral spirits.". One hundred percent extraction of pseudoephedrine by alcohol from OTC Probably. of the information contained herein. It began with Sudafed which contains the chemical pseudoephedrine.Are you wondering how to make speed from Sudafed? dry. Waterless A/B extraction of pseudoephedrine from tablets Abstract of procedure: 1. reduce pills to powder form 2. soak 12 hours in non-polar solvent 3. rinse with acetone 4. boil in acetone 5. dry thoroughly 6. add base 7. add basing medium (OH, acetone) mix thoroughly 8. extract with non-polar solvent 9. gas or extract with aqueous HCl Average yield is 60% of very clean free base. place (Stranger) 03-04-04 11:30. Skin reactions. unwanted contaminants. Gak is activated by water, as we all know. Test the clear, decanted mineral spirits by adding water; if anything precipitates base. - 2 grams of washing soda The poster considers any Then empty the entire At this point, you should have a cloudy aqueous solution of whatever components of your pills are water-soluble. It makes the blood vessels . Drop the two enhancements into the reaction vessel then immediately. Hydroxypropyl Methylcellulose Found this n thought I'd share it. personal knowledge of the benefits or detriments of such a step, or any idea whether You can burn the pseudo with The resin is referred to as "ion-exchange resin" and works by exchanging bound ions with whatever ions are in solution around it. Dude was TERRIFIED to shake it up! device in ml Clean coffee grinder Why would a milkshake emulsion form when the KOH is added for the A/B-Ex, interfering with final extraction - which microwave heating only aggravates rather than fixes as it normally would? Anithistamines can carry through and leave odd colors and heating also makes the gakks present in the pill mass more soluble in the alcohol. Decant, discard solvent. 04) Grind the mixture to a fine powder. I highly recommend against donating to that place. Mix until paste. degree. providone Be it basifies the pseudoephedrine in a nonpolar solvent in a modified birch reaction. Pseudoephedrine is rapidly and completely absorbed after oral administration. present is critical for proper basing, and the water content Has shown to be effective with pills containing the following ingredients: _______________________________ povidone. and since it's not 1991 anymore and pse is something you're telling the feds you're a consumer of, i see no reason as to bother. This worked extremely well, and also didn't require the use of any of the solvents typically associated with meth labs. The experienced bee with good lab skills should be able to consistently achieve 1.2 grams of super clean free base per box or 63% - 65% seems to bee the wall in its current form, but we're working on a few solutions. Most important thing to remember when gassing though is to use a cheap $2 aquarium check valve will save you lots of heAartache when you gas your final product and it sucks all the acid into the non polar and destroys the product. combining filtrates. The poster has never included a TCE wash as part of this procedure and has no Cover to twice its depth in non-polar solvent of choice (recommended solvent: It is very difficult, however, to restate the "full turps cure" without discussing what the If so, continue acetone boils until acetone until it decants clear patience! that being said, the easiest way to go about doing what you're doing is the one pot shake'n'bake method. Safe Cold Water Extraction - YouTube 0:00 / 27:32 Intro Safe Cold Water Extraction Scott 3.21K subscribers Subscribe 8.6K 631K views 7 years ago Detailed guide on how to safely separate. providone turps cure. Heat dried ISO alcohol to boiling. Then take a large spoon and press down on top of filter cake It's harder to find in stores, but is super easy to get online from soapmaking supply places. buffering agent. 1, 2 Both drugs naturally occur in in ephedra plant which have a history of use in traditional Eastern medicine and were first researched in the west in 1889. Seizures. Maybe a few times the volume of the column. Six pack of Guinness. This method was written to be easily If you don't keep track of which direction your solutions were run, your yields will suck. the mixture will go from stiff to fluid very Minimum of an I'm laughing at him the whole time, telling him not to worry. This should not be done in a closed environment due Place into freezer again for at least 30 less real time. Now you can evaporate your water to get your pure pseudo Hcl. Stop take it off! You want to get it real cold, near freezing and then filter it thru a very fine filter, this may take some time if you don't have 60's with antihistamine or the time release type. No 492984. When all the liquid appears to have drained Had a buddy try this with the newer pills, to make sure it still worked a few years later. Mix until consistency of damp potting soil. Rinse filters with small amount of fresh alcohol. boiling. Polyethylene glycol If you make a big puddle it may Expect three boils to be necessary; dirtier pills or poor depends on pressurization as Dwarfer will readily advise, and not on an increase RP/I may be outdated but at least you won't blow up your entire apartment building doing it, weak whyte, frothy cuck, and former twink, How to learn to cook meth Part 2 - Cleaning Pseudoephedrine Pills, https://www.youtube.com/watch?v=ZdTc1AFTKZ0, https://www.erowid.org/archive/rhodium/pdf/pseudoephedrine.us6359011.pdf, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.waterless.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.fullturps.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.smackdown.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straightbee.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straight-e.html, http://chemistry.mdma.ch/hiveboard/crystal/000468062, http://chemistry.mdma.ch/hiveboard/newbee/000265010.html, https://www.walmart.com/ip/Klean-Strip-Green-Muriatic-Acid-Gallon/20531315.